Experimental analysis of pure oxidesExperimental analysis of pure oxides as raw materials: Pb3 O4, TiO2, ZrO2, ZnO, Nb2O5, M nO2, Sb2 O3. According to the formula x Pb O3- y PbO3 - z PbTiO3 -, Pb ZrO3 + rM n, where is 0. 10 ~ 0. 20, y = 0. 020 ~ 0. 040, z =